High Resolution Transmission Electron Microscope Facility
Institute Of Physics,Bhubaneswar

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About the Facility


Machine:


1. Make : JEOL
2. Model:2010 (UHR version with URP 22 Polepiece)
3. Energy:200 keV
4. Electron Gun:LaB6
5. Vacuum Pumps:Rotary Pump, Diffusion Pump and Ion Pump
6. Resolution:(i) Point to Point : 0.19 nm (ii) Lattice : 0.14 nm
7. EDS: INCA (OXFORD)
8. Tilt Angles: Restricted to 15 deg maximum
9. Stages:(1) Double tilt Cryo stage (LN2 cooled) GATAN-636.
              (2) Single tilt Hot stage (upto 1000 Degree C ) GATAN-628 UHR.
10. Recording:(i) Conventional film camera
                     (ii) GATAN TV Camera-622
                    (iii) GATAN CCD Camera-832(4kX2k)
11. Data /Image acquisition with (i) DT3152 image grabber card
                                                (ii)Digital Micrograph


Sample Preparation:


(1) Grinder cum Polisher(SBT)
(2) Ultra Sonic Disc Cutter (GATAN)
(3) Dimple Grinder (GATAN)
(4) PIPS (Precision Ion Polishing System) (GATAN)
(5) Wire Saw (SBT)
(6) Tripod Polisher (SBT)
(7) Optical Microscope
(8) Low speed diamond wheel saw (from SBT)


Software:


(1) ImageJ (from NIH image analysis)
(2) WinHREM (Japan)
(3) SCION Image analysis
(4) Global Image (from DT)
(5) EDM (LDM/K)


Instruments For Sample Preparation


1.Grinder/Polisher (SBT)    2 : PIPS (Ion Milling) (GATAN)
3: Dimpler   4: Ultra Sonic cutter
5: Slow Speed Diamond Wheel Saw


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